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The stereoselective transformation from the commonly occurring 3α-bile acids and derivatives to their 3β-analogs is important for certain applications of these amphiphilic natural compounds, especially in the preparation of polymers. We report here the stereoselective conversion of methyl cholate to its 3β-hydroxy epimer by the use of the Mitsunobu reaction and to a 3β-amino cholic acid analog via...
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