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TiO2 and TiO2–V2O5 nanocrystals were prepared by coupling sol–gel and solvothermal methods, followed by heat-treatment at 400°C, after which the mean nanocrystal size was about 5nm. The materials were characterized by X-ray diffraction, transmission electron microscopy and solid state nuclear magnetic resonance spectroscopy. It was shown that while the TiO2 phase was always anatase even after heat-treatment...
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