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The rhodium(I) complex stabilised by the organometallic ligand 1,1'-bis(diphenylphosphino)ferrocene (dppf), [Rh(dppf) 2 ] + (1) can be electrochemically reduced to the Rh(0) and Rh(-1) species, [Rh(dppf) 2 ] (2) and [Rh(dppf) 2 ] - (3), respectively, in two reversible single-electron processes. These low-valent complexes have been obtained by the chemical reduction...
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