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The synthesis of 1,8-bis(dimethylaminomethylethynyl)-3,6-di(tert-butyl)fluorene-9-yl-acetic acid, a potentially dinucleating ligand containing two N-donor and bridging carboxylate groups, is described. The electronically disfavored 1,8-disubstitution of the fluorene ring system was achieved by using tert-butyl protecting groups in the 3- and 6-positions of the fluorene molecule in combination with...
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