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The Fujiwara hydroarylation of alkynes was reinvestigated using the addition of indole to methyl or ethyl phenylpropiolate catalyzed by Pd(OAc)2 as a model reaction. Reactions were monitored by both 1H NMR spectroscopy and electrospray ionization mass spectrometry (ESI/MS), and also through reactions carried out in the gas phase using MS/MS experiments. Contrary to the original suggestion for exclusive...
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