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An S-cyanocysteine-mediated α-carbon activation reaction was used for the block synthesis of unprotected peptides. The repeated reaction using the S-cyanocysteinyl peptides as building blocks made it possible to ligate several peptide segments in order to synthesize larger peptides with natural amide bonding.Segment ligation reaction of X-cyanocysteinyl peptide with unprotected peptide (R 2 ...
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