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Variable‐temperature FT‐IR spectra of poly(3‐hydroxybutyrate) (PHB), poly(ε‐caprolactone) (PCL) and a PHB/PCL (50:50 wt.%) blend were analyzed by two‐dimensional correlation spectroscopy (2DCOS). For this purpose the ν(CO) region was employed to characterize in some detail the crystallization behavior of the investigated polymer systems during cooling from the melt. The asynchronous 2D correlation...
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