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Thin films of polypyrrole were electropolymerised on a platinum electrode in electrolytes containing the small mobile chloride anion, the doubly charged sulfate anion and the bulky dodecyl benzene sulfonate (DBS) anion, and tested by in situ Raman spectroscopy using laser excitations of 488nm and 785nm. Cyclic voltammetry indicated that anion movement dominates the redox processes in a KCl electrolyte,...
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