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trans‐2,8‐Dioxabicyclodecane wurden in hohen Ausbeuten unter Aufbau von bis zu drei Stereozentren in einer säurevermittelten Eintopfreaktion aus γ,δ‐ungesättigten Alkoholen und Aldehyden synthetisiert (siehe Schema; Bn=Benzyl). Durch diese vielseitige Reaktion gelingt die stereoselektive Einführung von Substituenten an C3, C4, C7 und C9 des bicyclischen Gerüsts.
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