Syndiotactic polystyrene‐block‐poly(methyl methacrylate) copolymer is synthesized via the Huisgen 1,3 dipolar click cycloaddition reaction of properly end functionalized syndiotactic polystyrene (sPS) and poly(methyl methacrylate) (PMMA) polymer segments. The end functionalized sPS is obtained by quenching the styrene polymerization catalyzed by a half‐titanocene catalyst with N‐bromosuccinimide to...
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