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Cassava is an abundant and cheap source of starch which is largely used to produce sugar and dextrin. In this work, Hydrolysis of cassava starch using some active catalysts: poly(4‐vinylpyridine) hydrochloride (PVP, HCl), green clay activated with HCl, Amberlyst 36, Montmorillonite KSF, zeolite and HCl were investigated. Temperature, reaction time, concentration of starch and catalyst amount were...