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A series of symmetrically n‐alkyl‐substituted mono benzimidazolium salts with steady increase in n‐alkyl chain length have been prepared by stepwise N‐alkylation resulting in salts (1–8). The mono N‐heterocyclic carbene (NHC)–Ag(I) complexes (9–16) derived from the respective salts were readily accessible by in situ deprotonation using Ag2O. All the salts and the complexes were characterized using...
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