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Black red cauliflower-like microstructure films were synthesized by immersing copper foils in deionized water and ethanol component solvent (Vdeionized water: Vethanol = 1:1) solution of ammonia (DIWECSSA) at low temperature (0 − 25°C). The samples were characterized by SEM, EDX, XRD and TEM. Results showed that the black red film synthesized in 0.03M DIWECSSA at 25°C for 4h had novel cauliflower-like...
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