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A series of mercury(II) complexes, [Hg(NN)(SCN)2] (NN is 4,4′-dimethyl-2,2′-bipyridine in 1, 5,5′-dimethyl-2,2′-bipyridine in 2, 6,6′-dimethyl-2,2′-bipyridine in 3 and 6-methyl-2,2′-bipyridine in 4), were prepared from the reactions of Hg(SCN)2 with mentioned ligands in methanol. Suitable crystals of these complexes were obtained for X-ray diffraction measurement by methanol diffusion into a DMSO...