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This paper describes synthetic routes to produce highly 17 O enriched samples of the negative thermal expansion materials ZrW 2 O 8 and ZrMo 2 O 8 . In the case of ZrW 2 O 8 enriched samples can be produced either via enriched Zr 17 O 2 and W 17 O 3 , which have themselves been characterised by both X-ray diffraction...
Through-bond correlation NMR experiments have been used to characterize the structure of MP 2 O 7 crystalline compounds and disordered phosphates. For MP 2 O 7 materials, the refocused INADEQUATE experiment allows discrimination between the possible space group symmetries of the room temperature structure. The results show that the room temperature structure of ZrP...
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