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Bulk (MgB2)0.96Ni0.04 samples doping with premilled Ni powders were sintered at 750 °C for 30 min. During sintering, liquid Mg–Ni phase prompts solid–solid reaction between Mg and B and the size of milled Ni powder determines the final distribution of the secondary MgNi2.5B2 phase in the sintered samples. A flux jump was observed in the (MgB2)0.96Ni0.04 samples doping with Ni powders. Recognized from...
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