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In this study, hierarchical monoclinic BiVO 4 three-dimensional (3D) superstructures with two kinds of morphologies, namely BiVO 4 microboats and BiVO 4 microspheres, have been controllably synthesized by adjusting reaction time in the template-free hydrothermal process using ethylene glycol as solvent. The nucleation, growth, and self-assembly of the BiVO 4 superstructures...
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