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Ar‐BIANH2 bearing different substituents on the aryl rings have been synthesized in high yield by reduction of the corresponding bis(aryl)acenaphthenequinonediimine (Ar‐BIAN) compounds. The structure of p‐CH3C6H4‐BIANH2 in the solid state was determined by X‐ray diffraction. An exhaustive voltammetric investigation of the two parallel BIAN and BIANH2 series afforded a first rationalization of the...
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