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Six‐membered heterocycles, 1,4‐dithiane and 1,4‐thioxane, were treated with [Fe2(CO)6(μ‐pdt)] (pdt = propanedithiolate) in order to synthesise [2Fe3S] complexes with well positioned heteroatoms as potential base. Monosubstituted compounds of general formula [Fe2(CO)5L(μ‐pdt)] (L = 1,4‐dithiane, 1,4‐thioxane) were mainly obtained and characterised by 1H NMR, IR, elemental analysis and X‐ray diffraction...
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