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Although mononuclear complexes were mainly obtained from Cu2+ ion and phenyl‐, ethyl‐ or benzyl‐substituted thiazolo‐1,2,4‐triazine derivatives, unique metastable orange–yellow crystals [CuCl2(3a)]n (5a; Cu/3a = 1:1) with the phenyl‐substituted derivative 3a were obtained as a 1D coordination polymer through bis(μ‐chloro) linkages in a 2‐propanol solution. The crystals show dynamic and irreversible...
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