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Treatment of tri(2-aminoethyl)amine with three equivalents of BunLi followed by the addition of three equivalents of Ph3SiCl afforded the triaminoamine TrenTPSH3 [1, TrenTPSH3=N{CH2CH2N(H)SiPh3}3]. Subsequent treatment with three equivalents of BunLi afforded the tri-lithium complex [(TrenTPS)(Li)3] (2), which reacts with UCl4 to afford the uranium(IV) complex [U(TrenTPS)(Cl)] (3). Complex 3 is an...
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