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The self-assembly and photophysical properties of peptide-π-peptide molecules with ‘cruciform’ presentation of the π-electron core were studied. Derivatives of 1,4-bis(phenylethynyl)benzene were incorporated into a peptide backbone via the alkynylation of a central phenyl biscarboxamide core to yield peptide-π-peptide trimers wherein the π-conjugated unit was oblique to the peptide backbone. These...
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