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CO catalytic synthesis of diethyl carbonate in vapor phase had been studied in a continuous flow system and a fixed-bed reactor at atmospheric pressure. PdCl 2 –CuCl 2 /AC (activated carbon) catalyst exhibited better catalytic activity compared with other Wacker-type catalyst systems using SiO 2 , α-Al 2 O 3 and hexagonal mesoporous silica (HMS) as the carriers...
A vapor phase synthesis of diethyl carbonate (DEC) from carbon monoxide and ethyl nitrite (EN) was studied in a continuous flow micro fixed-bed reactor at atmospheric pressure. PdCl 2 –CuCl 2 /AC (activated carbon) catalyst exhibited better catalytic activity compared with other binary catalyst systems. The suitable Pd-loading is about 2.0 wt%, and some additives (LaCl 3 ,...
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