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Phase transition of water confined in nanospaces with charged inner‐surfaces was investigated by vibrational spectroscopy. Aerosol sodium bis(2‐ethylhexyl) sulfosuccinate (AOT) reverse micelles give a series of spherical nanospaces with controlled inner‐radius (Rw) with nanometer‐scale precision. Successive spectroscopic measurements of the confined water with decreasing temperature revealed that...
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