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Nano sized CoxNi1‐xFe2O4(0≤x≤1) samples were prepared by solution combustion method using glycine as fuel, maintaining a fuel to oxidizer ratio of 0.8. PXRD and FTIR analysis confirms the formation of the spinel phase. Non spherical and highly crystalline nature of the sample was revealed by HRTEM analysis. Lattice parameters of all samples calculated after Rietveld refinement and their variation...