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The exchange reactions of phosphorus dihalides RPX2 [R = iPr, cyclohexyl (Cy), tBu, (3,5‐Me2‐C6H3)CH2, Ph; X = Cl, Br], EtOPCl2, Et2NPCl2, Cl2PCH2PCl2, and Cl2PCH2CH2PCl2 with 2,2‐dimethyl‐4,5‐[1,2‐dicarba‐closo‐dodecaborano(12)]‐1,3‐diselena‐2‐silacyclopentane provide a straightforward route to 1,3,2‐diselenaphospholanes. Some tellurium analogues were prepared from the dilithium salt [1,2‐(LiTe)2...
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