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In contrast to the 2D organic‐inorganic hybrid Ruddlesden–Popper halide perovskites (RPP), a new class of 2D all inorganic RPP (IRPP) has been recently proposed by substituting the organic spacers with an optimal inorganic alternative of cesium cations (Cs+). Nevertheless, the synthesis of high‐membered 2D IRPPs (n > 1) has been a very challenging task because the Cs+ need to act as both spacers...
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