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Highly-crystallized cubic cattierite CoS2 pyramids were deposited on Ti foil via a simple hydrothermal method using CoCl2 and thiourea as precursors. Scanning electron microscopy (SEM) characterization revealed the morphology evolution from ramdom nanoparticles to micro-pyramids with well defined facets. These CoS2 pyramids were applied as electrocatalysts for hydorgen evolution reaction (HER) and...
A non-traditional electrodeposition technique carried out under the condition of electrolyte reduced-pressure surface-boiling is presented in this paper. Using this kind of technique, favorably smooth nickel coatings without pinholes and nodules are unexpectedly plated at a rate of up to 0.81mm/h from an additive-free bath. Analysis using SEM, TEM and XRD indicates that, microstructure and properties...
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