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Rapidly quenched amorphous Fe 80 Zr 4 Ti 3 Cu 1 B 12 (numbers indicate at.%) alloy was exposed to heat treatments in vacuum resulting in formation of a nanocrystalline structure with varying amounts of bcc-Fe grains. Mössbauer effect measurements were performed at 300 and 77K. An onset of crystallization was observed after annealing at 435°C for 1h. Analyses...