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Silver(I) salts demonstrate a strong preference for forming linear complexes when reacted with 4‐(phenylethynyl)pyridine (pep). The packing of these complexes was found to be strongly influenced by the counteranions, namely PF6–, BF4–, NO2–, NO3–, MeCO2–, CF3CO2–, MeSO3–, Tos– and SCN–. This study evaluates a family of twelve solid‐state structures that exhibit varying metal‐to‐ligand ratios, [Ag(pep)...
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