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A highly active and selective catalyst for light alkane oxidation that is composed of a pyridine salt of niobium-exchanged molybdo(vanado)phosphoric acid (NbPMo 11 (V)pyr) is characterized using TGA-DSC, 31 P MAS NMR, and in situ powder XRD, XAS, and XPS. The presence of both niobium and pyridinium species strongly influences structural and redox properties of the polyoxometalate...
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