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We have employed anomalous small angle X-ray scattering (ASAXS) and X-ray absorption in situ on an operating lithium ion battery cell with LiMn 2 O 4 as the positive electrode material. Manganese K-edge absorption spectra and scattering patterns were recorded at various stages of charge between 3.8 and 4.5 V. The shift of the manganese absorption K-edge was observed as a function of...
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