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The photoionization and dissociative photoionization of the allyl radical in the VUV range was investigated using synchrotron radiation. Allyl radicals were generated by flash pyrolysis from allyl iodide and 1,5-hexadiene. Mass spectra show the appearance of C 3 H 3+ as a fragment in the dissociative photoionization of allyl above 10eV. Between 10.4 and 10.5eV the C 3 ...
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