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The pyrolysis of polyborodiphenylsiloxane has been studied at temperatures up to 1600°C under an inert atmosphere. Above 1200°C both a nano-scale β-SiC and an amorphous phase developed while at temperatures greater than 1400°C significant mesoporosity started to appear, with surface areas and pore volumes reaching maximum values at around 1500°C. The porosity decreased at higher pyrolysis temperatures...
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