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The solvothermal synthesis of a novel mixed‐s‐block metal–organic framework is described, with crystallization brought about by use of the sodium salt of the benzo‐(1,2;3,4;5,6)‐tris(thiophene‐2′‐carboxylate) linker in combination with a lithium salt. The structure of the material was determined by single‐crystal X‐ray diffraction, which reveals an expanded version of the β‐cristobalite topology,...
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