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2,6-Diazidobiphenylene was synthesized and photolyzed in frozen matrix. The resulting electron spin resonance spectrum showed the formation of 2,6-biphenylenedinitrene as a quintet species with zero field splitting (zfs) parameters |D/hc|=0.260+/-0.002 cm -1 , |E/hc|=<0.0005 cm -1 . The zfs parameters are in excellent accord with dipolar models for a quintet state produced...
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