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The main goal of this study consisted in improving the performance of cementitious materials containing a percentage of rubber particles as a substitution for aggregates. Rubber surface was modified: new chemical and simple treatments based on calcium hydroxide or acetic acid solutions were applied. The effect of the above treatments was compared with that produced by sulphuric acid or sodium hydroxide...
An efficient stereocontrolled route to (±)-cylindricine C is described. Reaction of 9-hydroxynon-1-en-5-one oxime with 2,3-bis(phenylsulfonyl)-1,3-butadiene affords a 7-oxa-1-azanorbornane cycloadduct in high yield. The formation of the bicyclic isoxazolidine arises from conjugate addition of the oxime onto the diene to give a transient nitrone that spontaneously undergoes an intramolecular dipolar...
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