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In the present work, a new protocol for fast separation and quantification of JH III from biological samples using liquid chromatography coupled to electrospray tandem mass spectrometry is described. In particular, the proposed protocol improves existing methodologies by combining a limited number of sample preparation steps with fast LC-MS/MS detection, providing lower limits of detection and demonstrated...
Extracts of saw palmetto (Serenoa repens) fruits are used widely in the treatment of benign prostatic hyperplasia (BPH). This study presents an analysis of the fatty acid content of saw palmetto fruits from both the yellow-green and the less-distributed waxy blue-green forms growing in the Rockdale Pineland Preserve in Miami-Dade County, Florida. Extracts of the fruits were analyzed by GC and GC/MS...
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