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Dihydroxylation of styrene by chlorite (ClO2−) with scandium triflate [Sc(OTf)3] occurs efficiently to produce 1‐phenylethane‐1,2‐diol under the ambient conditions. Scandium triflate acting as a strong Lewis acid is found to accelerate the disproportionation of ClO2− to produce ClO− and ClO3−. A scandium‐chlorine dioxide complex (Sc3+ClO2•) is generated by the reaction of ClO− with ClO2− in the presence...
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