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Applications of double cross-polarization (CP) magic-angle spinning (MAS) NMR spectroscopy, via 1 H/ 15 N and then 15 N/ 13 C coherence transfers, for 13 C coherence selection are demonstrated on a 15 N/ 13 C-labeled N-acetyl-glucosamine (GlcNAc) compound. The 15 N/ 13 C coherence transfer is very sensitive to the settings of...
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