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Definitive experimental results on the geometry of fleeting species are at the time of writing still limited to monochromatic data collection, but methods for modifications of the polychromatic Laue data to increase their accuracy and their suitability for pump–probe experiments have been implemented and are reviewed. In the monochromatic experiments summarized, excited‐state conversion percentages...
New metastable species are formed by low-temperature irradiation of crystals of transition metal nitrosyl complexes. In the work described, photocrystallographic techniques, in which crystals are exposed in situ, are combined with differential scanning calorimetry measurements, IR spectroscopy and theoretical calculations. The new species are identified as isonitrosyl and η2-NO linkage isomers, which...
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