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Rotational-echo double-resonance (REDOR) 13 C NMR spectra with 2 H dephasing have been obtained from plaques and threads from the byssus of the marine musselMytilus edulislabeled by sea-water exposure tol-[ring-4- 13 C]tyrosine andl-[ring-d 4 ]tyrosine for 2 days. Specific isotopic enrichment of tyrosine in protein reached 25% in both 13 C and...
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