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Single crystals of the p‐type semiconductor CuAlO2, synthesized from the CuO flux method, have been investigated by electron paramagnetic resonance (EPR) spectroscopy at temperatures from 3.5 to 294 K. EPR spectra reveal an axial Cr3+ center and an axial Fe3+ center, presumably arising from impurities in the starting materials. The Cr3+ center at 294 K is characterized by g = 1.979(1) and D = − 7803(3)...
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