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In article number 2009949, Weibo Hua, Sylvio Indris, Laijun Liu, and co‐workers study the formation pathway of layered ordered LiNi0.6Co0.2Mn0.2O2 (O‐LNCM622O) from a mixture of precursor, Ni0.6Co0.2Mn0.2(OH)2 or Ni0.6Co0.2Mn0.2CO3, together with LiOH·H2O using in situ high‐temperature synchrotron radiation diffraction. A first‐order disorder‐to‐order transition from the disordered Li1−x(Ni0.6Co0.2...
Deciphering the sophisticated interplay between thermodynamics and kinetics of high‐temperature lithiation reaction is fundamentally significant for designing and preparing cathode materials. Here, the formation pathway of Ni‐rich layered ordered LiNi0.6Co0.2Mn0.2O2 (O‐LNCM622O) is carefully characterized using in situ synchrotron radiation diffraction. A fast nonequilibrium phase transition from...
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