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Hydrophobic nanoparticles were assembled into large-area monolayer films by combining oil/water interfacial self-assembly and phase separation of mixed ligands. Mixed ligands-capped nanoparticles were prepared simply by partially replacing the initial ligands of nanoparticle surfaces with polyvinylpyrrolidone (PVP). Infrared spectra and X-ray photoelectron spectroscopy demonstrate that O atom of PVP...
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