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The ordered double perovskites Sr2CrOsO6 and Ca2CrOsO6 have been synthesized and characterized with neutron powder diffraction, electrical transport measurements, and high field magnetization experiments. As reported previously Sr2CrOsO6 crystallizes with R3¯ symmetry due to a−a−a− octahedral tilting. A decrease in the tolerance factor leads to a−a−b+ octahedral tilting and P21/n space group symmetry...
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