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Mixed iron-gallium borate crystals Ga1−xFexBO3 have been studied by Magic Angle Spinning (MAS) NMR of 11B isotope. Experimental MAS NMR spectra have been computer simulated using a laboratory-developed code. The quadrupole parameters and isotropic chemical shift for 11B are consistent with threefold-coordination of boron atoms. A detailed fitting to the experimental NMR spectra reveals the existence...
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