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Intermetallic NixMy (M = Ga and Sn) nanocrystals with uniform particle size and controlled composition are successfully synthesized via a solution‐based co‐reduction strategy. The as‐obtained nanocrystals are crystalline and structurally ordered. The active‐site isolation and modified electronic structure are responsible for the excellent catalytic performance for alkyne semi‐hydrogenation of the...
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