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Vapor phase catalytic degradation of diethyl sulfide (DES) (simulant of sulfur mustard: a potential chemical warfare agent) at higher concentration (∼1200 ppm) was carried out in a fixed bed flow reactor over MnO/zeolite‐13X catalysts of different manganese contents. The catalytic process was studied in the temperature range of 100–400°C with air as the oxidizing agent. Process parameters such as...