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Ti3+ self-doped mesoporous black TiO2/SiO2 composite is successfully synthesized by a solvothermal reaction, followed by calcination at 450°C and hydrogenation at 500°C. The structures and morphologies of the resultant samples are investigated. The consequences suggest that Ti3+ self-doped mesoporous black TiO2/SiO2 composites have a high surface area of ∼300m2g−1, a relative large pore size of ∼4nm...
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